Seeing the Invisible

PolLux's X-Ray Vision Reveals the Nano-World

A revolutionary soft X-ray scanning transmission microscope at the Swiss Light Source

A New Era of Nanoscale Exploration

In the hidden universe of nanoscale structures—where materials exhibit exotic magnetic behaviors, polymers arrange in intricate patterns, and environmental particles reveal toxic secrets—conventional microscopes fall tragically short.

Revolutionary Technology

PolLux is a revolutionary soft X-ray scanning transmission microscope (STXM) at the Swiss Light Source (SLS), designed to map chemistry, magnetism, and structure with unprecedented precision.

Key Advantages

  • Unprecedented nanoscale resolution
  • Chemical fingerprinting capability
  • Magnetic state visualization
  • Versatile sample environments

PolLux at a Glance

PolLux's unique combination of capabilities enables breakthroughs across multiple scientific disciplines.

The Science Behind the Brilliance

Polarized Light as a Probe

PolLux exploits a fundamental principle: when soft X-rays (200–1,600 eV) strike matter, their absorption spectra act as a "chemical fingerprint." By tuning X-ray energy to specific atomic transitions (e.g., carbon K-edge at 284 eV), researchers identify molecular composition, bond orientation, and even magnetic states.

Unique to PolLux is its use of circularly polarized light, enabling real-time imaging of magnetic phenomena like skyrmions—nanoscale spin structures crucial for next-gen computing 1 8 .

Breaking the Diffraction Barrier

Unlike optical microscopes, PolLux uses Fresnel zone plates—concentric rings of metal—to focus X-rays into a nanometer-scale beam. As samples raster-scan through this beam, detectors measure transmitted X-rays, generating hyperspectral maps.

Recent upgrades achieved <20 nm resolution, revealing features 10,000x smaller than a human hair 1 6 .

Optical Microscopy
SEM
TEM
PolLux STXM

PolLux Technical Capabilities

Parameter Specification Scientific Impact
Energy Range 200–1,600 eV Covers K/L-edges of C, O, Fe, Co, Ni
Spatial Resolution <40 nm (currently ~20 nm) Resolves viruses, magnetic domains
Polarization Modes Linear, Circular (R/L) Probes chirality and magnetic textures
Sample Environment Vacuum to 1 atm (He/inert gas) Studies hydrated or reactive materials

Table 1: Comprehensive technical specifications of PolLux 1 2 6 .

Spotlight: Decoding 3D Magnetic Skyrmions

The Quest for Topological Stability

In 2025, an international team used PolLux to solve a persistent puzzle: how do magnetic skyrmions—whirlpool-like spin structures—maintain stability in three dimensions? These entities could revolutionize data storage but collapse under conventional imaging.

Experimental Breakthrough

  1. Sample Fabrication: The team grew freestanding antiferromagnetic nanomembranes of iron-germanium (FeGe), only 70 nm thick.
  2. Beamline Configuration: PolLux's fast helicity switching alternated left/right circularly polarized X-rays at the Fe L₃-edge (706 eV). This isolated magnetic signals from chemical backgrounds 2 8 .
  3. Laminography: Samples were tilted 60° and rotated, collecting 2D projections from multiple angles. Unlike tomography, this avoided sample shadowing.
  4. Reconstruction: Algorithms converted 2D data into a 3D vector field map, visualizing spin directions at each voxel (3D pixel) 2 .

Results & Implications

  • Skyrmions exhibited helical core structures winding through the membrane, not just surface spins.
  • Under electric fields, skyrmions reconfigured within nanoseconds, confirming them as low-energy data carriers.
  • Published in Nature Materials, this work established a roadmap for 3D spintronic devices 2 7 .
Skyrmion Experiment Parameters
Component Details
Sample FeGe nanomembrane (70 nm thick)
X-ray Energy 706 eV (Fe L₃-edge)
Polarization Rapid-switch circular (left/right)
Technique Soft X-ray laminography
Spatial Resolution 30 nm (in-plane); 50 nm (depth)

Table 2: Detailed parameters of the skyrmion imaging experiment 2 8 .

3D visualization of magnetic skyrmion structures revealed by PolLux's advanced imaging capabilities.

The Scientist's Toolkit: Inside PolLux's Innovation Arsenal

Zone Plates

Nanofabricated lenses focus X-rays. Current versions achieve <20 nm spots, with future upgrades targeting 10 nm 1 .

HOS Mirrors

Higher-Order Suppressor (HOS) Mirrors filter out stray high-energy photons, ensuring spectral purity 5 .

Ex Vacuo Movers

Reposition samples with <1 µm precision after environmental changes 8 .

Helicity Switching

Electron-beam steering allows sub-second polarization switching—critical for dynamic magnetic studies 1 .

Essential Research Reagents & Tools

Reagent/Tool Function
Circular Polarized X-rays Switchable helicity probes magnetic chirality
NEXAFS Spectroscopy Measures bond-specific absorption edges
TEY-STXM Detector Surface-sensitive electron yield imaging
Inert Gas Chamber Enables studies of air-sensitive nanomaterials

Table 3: Key components that enable PolLux's advanced capabilities 1 2 5 .

From Pollution to Polymers: PolLux's Versatility

Environmental Science

PolLux analyzed aerosol particles from urban air, identifying toxic heavy metals (e.g., lead) bound to organic residues. This revealed how pollutants evade lung clearance 4 .

Identification
Analysis
Mapping
Solution

Energy Materials

Using TEY-STXM, researchers confirmed homogeneous doping in organic solar cell nanoparticles. This ensured efficient charge transport, boosting device efficiency by 15% 2 .

Quantum Materials

Studies of superconducting cuprates mapped oxygen vacancy distributions, linking defects to quantum coherence loss 7 .

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Future Horizons: SLS 2.0 and Beyond

With the SLS 2.0 upgrade (2025), PolLux now delivers brighter beams, enabling multi-modal imaging (fluorescence + absorption) and faster nanoscale dynamics. The first post-upgrade user call is open for November 2025 beamtime 3 .

"Our next goal is 10 nm resolution—seeing single molecules in action."

Dr. Jörg Raabe, Lead Scientist

Conclusion: A Portal to the Nano-Cosmos

PolLux transcends traditional microscopy, merging chemistry, magnetism, and topology into a single vision. From stabilizing quantum states to tracking environmental toxins, it epitomizes how synchrotron science transforms abstract principles into tangible solutions. As it enters its SLS 2.0 era, this facility remains a beacon of what happens when human ingenuity illuminates the invisible.

For researchers:

Proposal deadlines for PolLux beamtime are August 20, 2025 (12:00 CET). Details: PSI Call Portal .

References